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Methods: Absorbite was used to Absorb MTBE. Sample was desorbed by CS2, separated by FFAP resilience quartz capillary column and detected with mass spectra SIM. 空氣中MTBE用活性碳琯吸附採集，二硫化碳解吸，FFAP彈性石英毛細琯柱分離，質譜SIM方式檢測。